Acta Pharm. 50 (2000) 29-37

Original scientific paper  
 

Determination of total flavonoids and quercetin in Hyperici herba and in its aqueous, aqueous-ethanolic and oil extracts

SVETLANA KULEVANOVA,1*   MARINA STEFOVA2 and  TRAJCE STAFILOV2

1Institute of Pharmacognosy, Faculty of Pharmacy, Skopje, Macedonia
2Institute of Chemistry, Faculty of Science, Skopje, Macedonia
Received July 14, 1999      Accepted February 14, 2000

Flavonoids of Hyperici herba (Hypericum perforatum L., Hypericaceae) collected in southwest Macedonia, were examined. The total flavonoid content determined spectrometrically (with AlCl3) was found to be 1.9%. The total flavonoid and total aglycone content varied in aqueous, aqueous-ethanolic and ethanolic extracts prepared from the same plant material. The highest value of total flavonoids (1.32 mg mL-1) was found in extracts obtained with 70% ethanol, whereas for total aglycones 50% ethanol was found to be the most effective extraction solvent giving 0.84 mg mL-1 aglycones. The content of total and aglycone quercetin was determined using HPLC. Its content in the plant material was found to be 1.3%. Analogously to flavanoids the highest value for total quercetin (0.68 mg mL-1 ) was also found in extracts prepared with 70% ethanol, and for aglycone 50% ethanol was most favorable and yielded 0.24 mg mL-1 quercetin. In olive oil extracts of Hyperici herba, highest yield of total flavonoids was obtained after three hours of digestion at 100 °C. Total flavonoids content in these oil extracts was 13.0 mg per 100 g.

Keywords: Hypericum perforatum L. (Hypericaceae), extracts, flavonoids, quercetin, spectrometry, HPLC